Kondenzační produkty 2-fenyl-1\kur{H}-imidazol-4-\nl{}-karbaldehydu s hydraziny

Ing. Daniel Cvejn

Master's thesis

Condensation products of 2-phenyl-1\kur{H}-imidazol-4-carbaldehyde with hydrazines

Abstract:

Práce je zaměřena na studium kondenzace syntetizovaného 2-fenyl-1\kur{H}-imidazol-4(5)-karbaldehydu s hydraziny. Bylo vyvinuto a otestováno několik postupů, s jejichž pomocí byly syntetizovány čtyři hydrazony. Identifikovány byly pomocí hmotnostní spektrometrie, NMR spektroskopie a infračervené spektroskopie. Experimentálně byly též prostudovány komplexační vlastnosti vznikajících látek. Cílové sloučeniny ani reakce, které k nim vedly, nebyly dosud v literatuře publikovány.

Abstract:

This thesis is concerned on study of condensation of synthesized 2-phenyl-1\kur{H}-imidazole-4(5)-carbaldehyde with hydrazines. Several protocols were developed and tested. Finally, four products were synthesized. Identification was realized by NMR spectroscopy, mass spectroscopy and IR spectroscopy. Complexation properties were experimentally studied too. The reaction protocols and target compounds have not been yet published in the literature.

Keywords

imidazol, aldehydy, hydraziny, hydrazony, komplexy

Language used: Czech

Date on which the thesis was submitted / produced: 5. 5. 2010

Thesis defence

• Date of defence: 1. 6. 2010
• Supervisor: Ing. Patrik Pařík, Ph.D.

University of Pardubice

Faculty of Chemical Technology

Master programme / field:
Chemistry / Organic Chemistry